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The fourth aliquot was analyzed via negative ionization following elution from a HILIC column (Waters UPLC BEH Amide 2.1 ร 150 mm, 1.7 ฮผm) using a gradient consisting of water and acetonitrile with 10 mM ammonium formate, pH 10.8
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Flow Rate:20 GPM
Kreher BW, Hennig J, Ilโyasov KA
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